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Ms.betty Ms.mayCAS NO.5794-88-7
comestic(1-25)Metric Toncomestic(25-100)Metric TonTop Grade (1-25)Metric Ton
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| CAS: | 5794-88-7 |
| MF: | C7H6BrNO2 |
| MW: | 216.03 |
| EINECS: | 227-338-3 |
| Product Categories: | Anilines, Amides & Amines;Bromine Compounds;Carboxylic Acids;Phenyls & Phenyl-Het;Benzoic acid series;Four-membered heterocyclic compound,Others;FINE Chemical & INTERMEDIATES;Amino Acids and Derivatives;Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts;Carboxylic Acids;Phenyls & Phenyl-Het;Benzoic acid;Organic acids;Acids & Esters;bc0001 |
| Mol File: | 5794-88-7.mol |
| 2-Amino-5-bromobenzoic acid Chemical Properties |
| Melting point | 213-215 °C (lit.) |
| Boiling point | 265.51°C (rough estimate) |
| density | 1.6841 (rough estimate) |
| refractive index | 1.6120 (estimate) |
| storage temp. | Keep in dark place,Inert atmosphere,Room temperature |
| solubility | Soluble in methanol and dimethyl sulfoxide. |
| form | Powder |
| pka | 4.55±0.10(Predicted) |
| color | Beige |
| Sensitive | Light Sensitive |
| Merck | 14,1405 |
| BRN | 639028 |
| CAS DataBase Reference | 5794-88-7(CAS DataBase Reference) |
| NIST Chemistry Reference | 2-Amino-5-bromobenzoic acid(5794-88-7) |
| 2-Amino-5-bromobenzoic acid Usage And Synthesis |
| Synthesis | A solution of bromine (7.2 g, 2 mL, 40 mmol) in 47 mL glacial acetic acid was added dropwise to sodium 2-aminobenzoate (6.4 g, 40 mmol) in 32 mL of glacial acetic acid at 15 °ะก and the mixture was stirred for 1 h at the same temperature. The product was filtered off, washed with benzene and dried in the dark. The bromobenzoic acids containing mixture (0.5 g) was added to 10 mL of boiling water followed by the addition of 1.3 mL of concentrated hydrochloric acid and hot filtration under vacuum. The insoluble material contained 2-amino-3,5-dibromobenzoic acid, whereas 2- amino-5-bromobenzoic acid precipitated upon cooling of the filtrate. IR (suspension in nujol, cm−1 ): 3497, 3383, 1675, 1616, 1587, 1548, 1423, 1377, 1316, 1292, 1239, 1160, 1127, 812, 748, 691. |
| Chemical Properties | slight yellow to white powder |
| Uses | 2-Amino-5-bromobenzoic acid is a brominated derivative of Antharilinic Acid (A679222). 2-Amino-5-bromobenzoic acid displays plant growth-regulator activity. 2-Amino-5-bromobenzoic acid is used in the preparation of hepatitis C virus NS5b RNA polymerase inhibitors. |
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